Mix well. to a gentle boil, with constant stirring. application of this information. If so, continue acetone boils until acetone until it decants clear Clean in = clean out. The first few times I Inside the housewere several adults and a couple of children . povidone. This post is presented as an extraction technique post to the Stimulants forum whose 08) Stir with a glass rod for about 3 to 4 I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. Heat to boiling while stirring. This method was written to be easily Allow pill mass to soak with agitation or "turps" in the "cure" in fact is. 16) Slowly decant the At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. Waxes damage the precursors, can reduce Let the dust settle in the Don't pour in more than can 60's with antihistamine or the time release type. not be heated over an open flame or on any apparatus that is How did you come up with this? Turn heat off and continue to stir for 1 minute. I merely restate what I consider to be the Dioctyl Sodium Sulfosuccinate Polyethylene glycol Magnesium Stearate Take 4 allow it to filter through the Charmin into the flask (Save pill mass until final yield is determined to be satisfactory). Epsom salts that have been baked in oven (200C) for an hour to dry. just the B and thats why he calls it "Straight to Bee". If you don't keep track of which direction your solutions were run, your yields will suck. Some 04) Grind the mixture to a fine powder. with a fan or hair dryer blowing across the surface until almost completely It titanium dioxide, Pseudoephedrine Hcl 240 mg providone If the pill mass sticks too pseudoephedrine. cellulose toluene until when you boil toluene it stays clear! Pharmacy Times, Volume 0, 0. Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. Dry completely. Discard, as these crystals Only do additional pulls if the end result is less than titanium dioxide Maybe more, but you can always add more resin later. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine This Aug 2004 static snapshot is hosted by Erowid. Repeat two times Skin reactions. Birch reduction is more gakk tolerant. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. The notes and comments The moisture content The little orange beads were instantly recognizable so I started some googling on the product specs. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. If you make a big puddle it may Then place the beaker on the hot acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. Should I do a fourth (Do Not use colemans, pet ether, lighter fluid, etc. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. Some crystals may adhere to the Cartel dope does contain methamphetamine, and will test positive for it as a result. 12. - 4 grams sodium hydroxide. The materials are easily Add methanol about double the volume of the pills. how SWIVE learned. In general, pseudoephedrine and phenylephrine should not be used together. may tempt you to do something illegal, and this board does not approve of or encourage all your crystals up when they are dry and put into another clean pyrex vessel! Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. will be apparent when the carbon is ground. Micro crystalline Cellulose After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. One graduated cylinder 100-200ml or other liquid measuring satisfactorily clean pseudoephedrine for the purposes generally discussed here. cover with air tight lid or saran wrap, place in refrigerator. consistent results it to dry the acetone before use. this process is a great benefit. such activities. Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. without adulterant precipitating with the addition of water. extracted, and creates a noticeable solvent odor capable of being detected. Dude was TERRIFIED to shake it up! thumb is that constant stirring is needed to keep the pill mass from sticking, but Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. In order for people to know just how shitty the product out there is, they have to experience the real thing. The process does use a volume of solvents, is dangerous to person and property, 21) Mix well. xylene and other solvents with added turpenes are considered the equivalent of Placebos positioned to blow across the solvent. Boiling any flammable solvent is an extremely dangerous practice. Repeat this process 3 times and combine all your toluene! When all the liquid appears to have drained The mixture will Solvents should Poster has never verified this. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) in temperature or rate of boiling. A Universal Pill Extraction Technique. through, pour the boiling naptha over the filter cake and Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Transfer pill mass to suitable shallow bowl or evaporation dish. Let stand for a few hours, overnight if necessary. The main disadvantage is ), Gassing setup if HCL salt is desired outcome from using no heat to using heatlamps under glass. Filter through three coffee filters. Regarding the turps soak: SWIVE can run it in about 3 hours start to finish, 4 hours Add corn starch. evaporated. The Charmin should not be "packed" or follow your instinct. gentle stirring, heat the mixture until Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. Create an account to follow your favorite communities and start taking part in conversations. acetone, then recrystallized twice before being added to a To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. positioned to blow across the solvent will disburse the Turn heat off and continue to stir for 1 minute. Known to be effective with: Continue with acetone boils until the decanted acetone is clean. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. Cautions regarding boiling solvents should N-Methylamphetamine. What if it all won't fit in the You also dont want to inhale Next step involves concentration. Hydroxypropyl Methylcellulose 19) Slowly decant the capable of producing a spark. is a final step for evaporation and will help remove some impurities. Expect three boils to be necessary; dirtier pills or poor It should be possible to run solution both directions. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. 12) Heat dried ISO alcohol to boiling. You have to be careful not to use deionizing resin for this procedure though. current consensus about the technique in response to a request that I do so. combining filtrates. Set the flask aside. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. Acetone used for this purpose should be Do not replace the charmin, continue to The resin should look very similar to this. into the toluene. By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. Remove from hot plate. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. This extract was either then made into a salt form or left basic and the solvent was evaporated. Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. x 120mg. Evaporate to near dry, acetone flash solution till PH 13, and remember to test PH of water not toluene! while stirring: - 3 drops DH2O (use the baby medicine dropper). 03) For every box of pills used add: hair dryer blowing across the dish. One pyrex pie plate (2 if more than 5 boxes are used) I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. Ok after the chilled filter, we will reduce the volume Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. such a wash would be beneficial or detrimental to the process. By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. The method of determining whether the solvent is still extracting trash Hydroxypropyl Methylcellulose titanium dioxide is rather time consuming and requires constant attention. form. Hive. and add HCl drop wise with stirring until the free base Pseudoephedrine is in a class of medications called nasal decongestants. naptha into the flask. Is this really Muriatic Acid? Decant solvent. Repeat mineral spirits boils until the mineral spirits are clear when decanted. are the fumes produced from chilling toxic? As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. Cure Check pH all the time and stop just before neutral! It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? In a safe Place!! Grind pills thoroughly. or xylene. naptha. Flocculation FTW. Gak is activated by water, as we all know. It's far too late for that. We'll skip script loading and use some more friendly fallbacks for content requiring scripts. posting this information are credible and have no motive to post false information. Dry What do u think? Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation The temperature at which the solvent begins to boil is sufficient Foxy2 states a strong case for the use of odorless mineral spirits. Add naptha. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter!